Endocrine-disrupting compounds surveying in polyethylene packed injection solutions using microwave-accelerated air-assisted liquid–liquid microextraction based on solidification of deep eutectic solvent
Endocrine-disrupting compounds surveying in polyethylene packed injection solutions using microwave-accelerated air-assisted liquid–liquid microextraction based on solidification of deep eutectic solvent
نویسندگان: محمدرضا افشار مقدم , محبوب نعمتی
کلمات کلیدی: Endocrine-disrupting
compounds; air-assisted
liquid–liquid
microextraction; injection
solutions; gas
chromatography; mass
spectrometry
نشریه: 31442 , 0 , 0 , 2020
| نویسنده ثبت کننده مقاله |
محمدرضا افشار مقدم |
| مرحله جاری مقاله |
تایید نهایی |
| دانشکده/مرکز مربوطه |
مرکز تحقیقات ایمنی غذا و دارو |
| کد مقاله |
73939 |
| عنوان فارسی مقاله |
Endocrine-disrupting compounds surveying in polyethylene packed injection solutions using microwave-accelerated air-assisted liquid–liquid microextraction based on solidification of deep eutectic solvent |
| عنوان لاتین مقاله |
Endocrine-disrupting compounds surveying in polyethylene packed injection solutions using microwave-accelerated air-assisted liquid–liquid microextraction based on solidification of deep eutectic solvent |
| ناشر |
4 |
| آیا مقاله از طرح تحقیقاتی و یا منتورشیپ استخراج شده است؟ |
بلی |
| عنوان نشریه (خارج از لیست فوق) |
|
| نوع مقاله |
Original Article |
| نحوه ایندکس شدن مقاله |
ایندکس شده سطح یک – ISI - Web of Science |
| آدرس لینک مقاله/ همایش در شبکه اینترنت |
|
| A green and centrifuge-less microwave-accelerated air assisted liquid–liquid microextraction
method based on solidification of deep eutectic solvent droplet has been developed for the
extraction of some endocrine-disrupting compounds in injection solutions prior to their determination by gas chromatography–mass spectrometry. Under optimum conditions, limits of detection
and quantification were obtained in the ranges of 14–33 and 47–110 ng L–1, respectively. Extraction
recovery (ER) and enrichment factor (EF) of the selected analytes ranged from 79% to 94% and
395–470, respectively. The relative standard deviations were ≤7% for intra- (n = 6) and inter-day
(n = 4) precisions at a concentration of 250 ng L–1 of each analyte. |
| نام فایل |
تاریخ درج فایل |
اندازه فایل |
دانلود |
| endocrin-disrupt-int.pdf | 1399/07/14 | 3009977 | دانلود |
