Determination of 105 Pesticides in Vegetables and Lettuce using QuEChERS Sample Preparation Method and Gas Chromatography and Mass Spectrometry

Determination of 105 Pesticides in Vegetables and Lettuce using QuEChERS Sample Preparation Method and Gas Chromatography and Mass Spectrometry


چاپ صفحه
پژوهان
صفحه نخست سامانه
نویسندگان
نویسندگان
اطلاعات تفضیلی
اطلاعات تفضیلی
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دانشگاه علوم پزشکی تبریز
دانشگاه علوم پزشکی تبریز

نویسندگان: محمدعلی تربتی , علی اکبر علیزاده , سولماز عابدین زاده تیمورلویی

عنوان کنگره / همایش: چهاردهمین همایش سراسری سم شناسی ایران , Iran (Islamic Republic) , شیراز , 2017

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نویسنده ثبت کننده مقاله محمدعلی تربتی
مرحله جاری مقاله تایید نهایی
دانشکده/مرکز مربوطه دانشکده تغذیه
کد مقاله 68243
عنوان فارسی مقاله Determination of 105 Pesticides in Vegetables and Lettuce using QuEChERS Sample Preparation Method and Gas Chromatography and Mass Spectrometry
عنوان لاتین مقاله Determination of 105 Pesticides in Vegetables and Lettuce using QuEChERS Sample Preparation Method and Gas Chromatography and Mass Spectrometry
نوع ارائه پوستر
عنوان کنگره / همایش چهاردهمین همایش سراسری سم شناسی ایران
نوع کنگره / همایش ملی
کشور محل برگزاری کنگره/ همایش Iran (Islamic Republic)
شهر محل برگزاری کنگره/ همایش شیراز
سال انتشار/ ارائه شمسی 1396
سال انتشار/ارائه میلادی 2017
تاریخ شمسی شروع و خاتمه کنگره/همایش 1396/08/02 الی 1396/08/04
آدرس لینک مقاله/ همایش در شبکه اینترنت
آدرس علمی (Affiliation) نویسنده متقاضی 1Department of Food Science and Technology, Faculty of Nutrition, Tabriz University of Medical Sciences, Tabriz, Iran.

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نویسنده نفر چندم مقاله
محمدعلی تربتیاول
علی اکبر علیزادهسوم
سولماز عابدین زاده تیمورلوییاول

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عنوان متن
کلمات کلیدیPesticide Residues; QuEChERS; Gas Chromatography, Mass Spectrometry
خلاصه مقالهAbstract Farmers use a large number of pesticides to control pest and diseases which damage their plants. The presence of pesticide residues in the vegetable and lettuce are important concern not only for consumers, but also for the Iranian regulatory authorities, due to popular use of vegetables and lettuce in daily meal of Iranian. To determine residual amounts of pesticides in the vegetable and lettuce we used a rapid, specific and sensitive multipurpose method based on the modified Quick Easy Cheap Effective Rugged and Safe (QuEChERS) sample preparation and gas chromatography with electron mass spectrophotometer. In this method based on ion monitoring mode (GC–MS-SIM) one or two qualified ions were selected for routine analysis of 105 pesticides in vegetables and lettuce. The recovery method for all studied pesticides was from 75.6% to 89.5% and in the concentration range of 0.002–0.15 mg/kg. This method was successfully used for analysis of remaining pesticides in supplied vegetables and lettuce in the fruit and vegetable markets. In comparison with limit allowed of National Standards Organization, our results showed that 5.71% and 10% of unwashed vegetables and lettuce respectively were rejected from the point of remaining pesticides. The Iprodine, Kersoxim-methyl and Diazinon toxins were the main residual pesticides in the rejected samples. By consideration of the carence period of each pesticide and proper cleaning of agricultural products we can minimize the residue of pesticides and reduce their health risks.

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